Page 8

ACE Food & Beverage Applications Guide-Hichrom

Pesticides by LC-MS/MS Conditions Column: ACE UltraCore 2.5 SuperC18 Dimensions: 50 x 2.1 mm Part Number: CORE-25A-0502U Mobile Phase: A: 0.1% formic acid + 5 mM ammonium formate in H2O/MeOH (90:10 v/v) B: 0.1% formic acid + 5 mM ammonium formate in H2O/MeOH (10:90 v/v) Flow Rate: 0.4 mL/min Injection: 20 μL Temperature: 40 °C Detection: Agilent 6420 Triple Quadrupole MS, +ve mode ESI Dynamic MRM Application #AN1290 1. Carbaryl (m/z 202.10 → 145.10) 2. Dimethomorphs (m/z 388.10 → 301.10) 3. Cyproconazoles (m/z 292.10 → 70.00) 4. Fenbuconazole (m/z 337.10 → 70.00) Time (mins) %B 0.00 0 1.00 0 15.00 100 18.00 100 18.05 0 20.00 0 1 2 3 4 Also analysed under same conditions: Acephate, Acetamiprid, Aldicarb, Aldicarb sulfone, Aldicarb sulfoxide, Benomyl, Carbendazim, Carbofuran, Clofentezine, Clothianidin, Cyfluthrin, Demeton S-methylsulfone, Demeton S-methylsulfoxide, Dicrotophos, Dimethoate, Dinotefuran, DMA, DMPF, Flubendiamide, Folpet, Formetanate, Hexaconazole, Hexaflumuron, Imidacloprid, Indoxacarb, Mandipropamid, Methamidophos, Methomyl, Monocrotophos, Nicotine, Omethoate, Oxamyl, Pencycuron, Prochloraz, Propargite, Thiabendazole, Thiacloprid, Thiamethoxam, Thiodicarb, Thiophanate methyl and Triforine Reproduced with permission of Kent Scientific Services 6


ACE Food & Beverage Applications Guide-Hichrom
To see the actual publication please follow the link above