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ACE Food & Beverage Applications Guide-Hichrom

Mycotoxins by LC-MS/MS 7.5e5 7.0e5 6.5e5 6.0e5 5.5e5 5.0e5 4.5e5 4.0e5 3.5e5 3.0e5 2.5e5 2.0e5 1.5e5 1.0e5 5.0e4 4 2 1 3 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 6.5 0 min cps Conditions Column: ACE Excel 2 C18-AR Dimensions: 50 x 2.1 mm Part Number: EXL-109-0502U Mobile Phase: A: 1 mM ammonium acetate, 0.5% acetic acid in H2O B: 1 mM ammonium acetate, 0.5% acetic acid in 95% MeOH Flow Rate: 0.6 mL/min Injection: 2 μL Temperature: 40 °C Detection: AB SCIEX triple quad 5500 Positive ESI mode Source temperature: 500 °C IonSpray voltage: 5500 V Application #AN2330 1. Aflatoxin G2 (m/z 331.1 313.1) 2. Aflatoxin G1 (m/z 329.0 243.1) 3. Aflatoxin B2 (m/z 315.1 287.0) 4. Aflatoxin B1 (m/z 313.1 285.0) 5. HT-2-toxin (m/z 442.2 263.1) 6. T-2-toxin (m/z 484.2 305.1) 7. Ochratoxin A (m/z 404.1 239.0) Time (mins) %B 0.0 40 1.0 40 2.4 60 6.8 87 Reproduced with permission of Biotage GB Ltd 5 6 7 42


ACE Food & Beverage Applications Guide-Hichrom
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