ACE UHPLC and HPLC Columns
Perfluorinated Compounds in Water by LC-MS/MS
122
• Highly cost effective - 2 and 3 column kits
available for the same price as a single column
• 4 different Method Development Kits available in
dimensions from microbore (0.5 mm id) through
to analytical (4.6 mm id) for rapid, systematic
method development.
• Carefully selected ACE phases enabling the power
of selectivity to be fully exploited
• Each ACE phase provides different selectivity due
to differing interactions
ACE
Method Development Kits
Intelligent Solutions for
Method Development
• UHPLC and HPLC method development kits
• Kits available from microbore to analytical dimensions
• Porous, solid-core and biomolecule options
• Wide range of particle sizes and complementary phases available
• Excellent peak shape, efficiency, reproducibility and lifetime
• Highly cost effective
ACE
UHPLC and HPLC Columns
www.ace-hplc.com | +44 (0) 1224 704 554 | info@ace-hplc.com
1
2
3
4
5
6
7
Column: ACE Excel 1.7 C18
Dimensions: 100 x 2.1 mm
Part Number: EXL -171-1002U
Mobile Phase: A: 2 mM ammonium
acetate, 0.1% formic acid in
H2O/MeCN (90:10 v/v)
B: 2 mM ammonium
acetate, 0.1% formic acid in
H2O/MeCN (10:90 v/v)
Gradient: Time (mins) %B
0.0 25
0.5 25
3.5 70
4.0 100
5.5 100
6.0 25
9.0 25
Flow Rate: 0.5 mL/min
Injection: 10 μL
Temperature: 40 °C
Detection: AB SCIEX triple quad 5500
Negative ESI MRM
Source temperature: 450 °C
IonSpray voltage: -2400 V
Application #AN2260
Conditions Analytes
1. Perfluorohexanoic acid
(m/z 313.0 268.9)
2. Perfluorobutanesulfonic acid
(m/z 299.0 79.9)
3. Perfluorooctanoic acid
(m/z 413.0 368.9)
4. Perfluorohexanesulfonic acid
(m/z 399.0 80.0)
5. Perfluorononanoic acid
(m/z 463.0 419.0)
6. Perfluorodecanoic acid
(m/z 513.0 469.0)
7. Perfluorooctanesulfonic acid
(m/z 499.0 80.0)
Time - Minutes
Reproduced with permission of Biotage GB Ltd, UK. For extraction conditions see Biotage Application Note AN839
ACE Method Development Kits
Intelligent Solutions for Method Development
FREE Application Support and FREE Method Development Service
Learn more: www.ace-hplc.com or email: info@ace-hplc.com
products are available through
international network of distributors
Offer:
kits
price
Selectivity column same the column
and 3 for single available 2 as a